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Studies of stoichiometric hydroformylation, spectroscopic identification, isolation, and transformation of intermediates provided valuable information of the understanding of the catalytic reaction. Despite the complexity of the process, important conclusions were also drawn from kinetic studies. Evidence was presented that cobalt precursors under the reaction conditions are transformed into cobalt carbonyls 1 Additives such as Lewis bases accelerate the formation of the catalyst. II [COH(CO)4] the key catalytic species was shown by infrared (IR) spectroscopy to be formed under hydroformylation conditions32 and was isolated in the reaction of [Co(CO)4h and hydrogen 3 [COH(CO)4] dissociates carbon monoxide to create [CoH(COh] [Eq. 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